2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan

Base Information

• Chemical Name: 2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan
• CAS No.: 102276-72-2
• Molecular Formula: C₁₅H₂₁BrO₃
• Molecular Weight: 329.234
• Mol file: 102276-72-2.mol

Synonyms:2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan

Chemical Property of 2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan

There total 1 articles about 2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-bromo-1-(4-methoxyphenyl)-1-propanone (21086-33-9) + 2,2-Dimethyl-1,3-propanediol (126-30-7) → 2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan (102276-72-2)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; Heating;

DOI:10.1055/s-1985-31249

Reference yield:

2-(1-bromoethyl)-5,5-dimethyl-2-(4-methoxyphenyl)-1,3-dioxan (102276-72-2) → 2-(4-methoxyphenyl)propanoic acid (942-54-1)

Guidance literature:

With sodium hydroxide; potassium acetate; Yield given. Multistep reaction; 1.) 1,2-ethanediol, 125 deg C, 8 h, 2.) MeOH, reflux, 4 h;

DOI:10.1055/s-1985-31249

upstream raw materials:

2-bromo-1-(4-methoxyphenyl)-1-propanone

2,2-Dimethyl-1,3-propanediol

Downstream raw materials:

2-(4-methoxyphenyl)propanoic acid