2,6-dimethyl-2-nitrophenyl azide

Base Information

• Chemical Name: 2,6-dimethyl-2-nitrophenyl azide
• CAS No.: 862307-78-6
• Molecular Formula: C₈H₈N₄O₂
• Molecular Weight: 192.177

Synonyms:2,6-dimethyl-2-nitrophenyl azide

Chemical Property of 2,6-dimethyl-2-nitrophenyl azide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2,6-dimethyl-2-nitrophenyl azide

There total 2 articles about 2,6-dimethyl-2-nitrophenyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2,4-Dimethyl-6-nitroanilin (1635-84-3) → 2,6-dimethyl-2-nitrophenyl azide (862307-78-6)

Guidance literature:

With hydrogenchloride; sodium azide; sodium nitrite; In water; at -5 - 25 ℃;

DOI:10.1002/hlca.200590126

Reference yield:

→ 2,6-dimethyl-2-nitrophenyl azide (862307-78-6)

Guidance literature:

With ammonia;

Reference yield:

1,4-Dihydro-1,4-dimethyl-5-(1-methylethyliden)-5H-tetrazol (54986-15-1) + 2,6-dimethyl-2-nitrophenyl azide (862307-78-6) → 5-{1-[3-(2,4-dimethyl-6-nitrophenyl)triaz-1-enyl]-1-methylethyl}-1,4-dimethyl-1H-tetrazolium inner salt

Guidance literature:

In dichloromethane-d2; at -75 ℃;

DOI:10.1002/hlca.200590126

upstream raw materials:

2,4-Dimethyl-6-nitroanilin

Downstream raw materials:

4,6-Dimethylbenzfuroxan

3,5-dimethyl-[1,2]benzoquinone dioxime

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