2,5-Dichloro-1,3-dinitrobenzene

Base Information

• Chemical Name: 2,5-Dichloro-1,3-dinitrobenzene
• CAS No.: 2213-82-3
• Molecular Formula: C6H2 Cl2 N2 O4
• Molecular Weight: 236.999
• Hs Code.: 2904909090
• European Community (EC) Number: 218-673-6
• NSC Number: 67758
• UNII: 32VX4DFV3R
• DSSTox Substance ID: DTXSID6062256
• Nikkaji Number: J80.429K
• Wikidata: Q27256195
• Mol file: 2213-82-3.mol

Synonyms:2,5-Dichloro-1,3-dinitrobenzene;2213-82-3;1,4-Dichloro-2,6-dinitrobenzene;2,6-Dinitro-1,4-dichlorobenzene;UNII-32VX4DFV3R;Benzene, 2,5-dichloro-1,3-dinitro-;32VX4DFV3R;EINECS 218-673-6;NSC 67758;NSC-67758;NSC67758;2,3-dinitrobenzene;SCHEMBL9452603;DTXSID6062256;Benzene,5-dichloro-1,3-dinitro-;2,5-dichloro-1,3-dinitro-benzene;A1-02815;Q27256195

Chemical Property of 2,5-Dichloro-1,3-dinitrobenzene

Chemical Property:

• Vapor Pressure: 0.000793mmHg at 25°C
• Melting Point: 105 °C
• Boiling Point: 315.8°Cat760mmHg
• Flash Point: 144.8°C
• PSA: 91.64000
• Density: 1.729g/cm³
• LogP: 3.85620
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 235.9391619
• Heavy Atom Count: 14
• Complexity: 227

Purity/Quality:

99% up ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C=C(C(=C1[N+](=O)[O-])Cl)[N+](=O)[O-])Cl

Technology Process of 2,5-Dichloro-1,3-dinitrobenzene

There total 20 articles about 2,5-Dichloro-1,3-dinitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

para-dichlorobenzene (106-46-7,84348-21-0) → 1,4-dichloro-2,5-dinitrobenzene (17488-25-4) + 2,5-dichloro-1,3-dinitrobenzene (2213-82-3) + 1,4-dichloro-2,3-dinitrobenzene (65036-57-9)

Guidance literature:

With sulfuric acid; nitric acid; at 70 ℃; for 4h;

Reference yield: 3.0%

1-chloro-2,6-dinitrobenzene (606-21-3) → 2,4,6-trinitrochlorobenzene (88-88-0) + 2,5-dichloro-1,3-dinitrobenzene (2213-82-3)

Guidance literature:

With sulfuric acid; nitric acid; at 130 ℃; for 0.666667h;

Reference yield:

para-dichlorobenzene (106-46-7,84348-21-0) → 2,5-dichloro-1,3-dinitrobenzene (2213-82-3)

Guidance literature:

With sulfuric acid; nitric acid;

upstream raw materials:

para-dichlorobenzene

4-chloro-2,6-dinitroaniline

4-chloro-2,6-dinitrophenol

p-toluenesulfonyl chloride

Downstream raw materials:

2,6-dinitro-4-chloroanisole

4-chloro-2,6-dinitroaniline

3-(4-chloro-2,6-dinitro-phenyl)-2-thioxo-thiazolidin-4-one

2'-Brom-,4-chlor-2,6-dinitro-diphenylsulfid

Refernces

• 1、 Page,Heasman. "-". . p. 3247. Retrieved 1923.
• 2、 Huwe,Feil,Larsen,Wiener. "Metabolism and disposition of 1,4,7,8-tetrachlorodibenzo-p-dioxin in rats". . p. 1885 - 1893. Retrieved 2007/10/03.
• 3、 Melhuish, Martin W.,Moodie, Roy B.. "Electrophilic Aromatic Substitution. Part 35. Chlorination of 1,3-Dinitrobenzene, 1-Chloro-2,4-dinitrobenzene, and 2,4-Dinitrotoluene with Nitric Acid and Hydrogen Chloride or Chlorine in Sulphuric Acid or Oleum". . p. 667 - 674. Retrieved 2007/10/02.