Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

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Chemical Name:Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester
CAS No.:847949-32-0
Molecular Formula:C₂₅H₃₃BrO₄
Molecular Weight:477.439
Hs Code.:

Synonyms:Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

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Chemical Property of Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

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Technology Process of Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

There total 5 articles about Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (3S,4S)-3-[2,6-diacetoxy-4-pentylphenyl]-2-acetoxy-4-isopropenyl-1-methylenecyclohexane

: 847949-32-0
Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

Guidance literature:: With trimethylsilyl bromide; zinc(II) iodide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/b416943c

Reference yield:

: 247227-98-1,22198-90-9
(1S,2S)-2',6'-dimethoxy-5-methyl-4'-pentyl-2-(prop-1-en-2-yl)-1,2,3,4-tetrahydro-1,1'-biphenyl

: 847949-32-0
Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / 0 °C

2: 97 percent / BuLi; N-cyclohexylisopropylamine; methylmagnesium bromide / toluene; diethyl ether / 2 h / 40 °C

3: 42 percent / MeMgI / diethyl ether / 0.75 h / 210 °C

4: 100 percent / pyridine / 18 h / 20 °C

5: 90 percent / TMSBr; ZnI₂ / CH₂Cl₂ / 4 h / 20 °C

With pyridine; methyl magnesium iodide; n-butyllithium; trimethylsilyl bromide; N-cyclohexylisopropylamine; methylmagnesium bromide; 3-chloro-benzenecarboperoxoic acid; zinc(II) iodide; In diethyl ether; dichloromethane; toluene;
DOI:10.1039/b416943c

Reference yield:

: 847949-24-0
(1R,4S,5S,6S)-5-(2,6-Dimethoxy-4-pentyl-phenyl)-4-isopropenyl-1-methyl-7-oxa-bicyclo[4.1.0]heptane

: 847949-32-0
Acetic acid 3-acetoxy-2-((1S,6S)-3-bromomethyl-6-isopropenyl-cyclohex-2-enyl)-5-pentyl-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / BuLi; N-cyclohexylisopropylamine; methylmagnesium bromide / toluene; diethyl ether / 2 h / 40 °C

2: 42 percent / MeMgI / diethyl ether / 0.75 h / 210 °C

3: 100 percent / pyridine / 18 h / 20 °C

4: 90 percent / TMSBr; ZnI₂ / CH₂Cl₂ / 4 h / 20 °C

With pyridine; methyl magnesium iodide; n-butyllithium; trimethylsilyl bromide; N-cyclohexylisopropylamine; methylmagnesium bromide; zinc(II) iodide; In diethyl ether; dichloromethane; toluene;
DOI:10.1039/b416943c