tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

Base Information

Chemical Name:tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide
CAS No.:1397683-33-8
Molecular Formula:C₁₄H₁₈N₂O₇S
Molecular Weight:358.372
Hs Code.:

Synonyms:tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

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Technology Process of tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

There total 7 articles about tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1397683-33-8
tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

Guidance literature:

Reference yield:

: 1397683-93-0
C₁₄H₁₈N₂O₆S

: 1397683-33-8
tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

Guidance literature:: With sodium periodate; ruthenium trichloride; In water; acetonitrile; at 0 - 20 ℃; for 2h;

Reference yield:

: 1270385-54-0
rac-2-amino-2-(3-nitro-phenyl)-propan-1-ol

: 1397683-33-8
tert-butyl 4-methyl-4-(3-nitrophenyl)-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran / 15 h / 0 - 20 °C

2: thionyl chloride; pyridine / acetonitrile / 18.5 h / -40 - 20 °C / Inert atmosphere

3: sodium periodate / ruthenium trichloride / acetonitrile; water / 2 h / 0 - 20 °C

With pyridine; sodium periodate; thionyl chloride; sodium hydrogencarbonate; ruthenium trichloride; In tetrahydrofuran; water; acetonitrile;