ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

Base Information

Chemical Name:ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate
CAS No.:1168134-88-0
Molecular Formula:C₁₇H₂₂BrClO₄
Molecular Weight:405.716
Hs Code.:

Synonyms:ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

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Chemical Property of ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

Chemical Property:

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Technology Process of ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

There total 4 articles about ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1168133-69-4
ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)acetate

: 6482-24-2
2-Bromoethyl methyl ether

: 1168134-88-0
ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

Guidance literature:: ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)acetate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

2-Bromoethyl methyl ether; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

Reference yield:

: 193357-36-7
3-chloro-4-hydroxyphenylacetic acid ethyl ester

: 1168134-88-0
ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine / chloroform / 1 h / 0 °C

2.1: potassium carbonate / dimethyl sulfoxide / 4 h / 60 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

3.2: 0.5 h / 0 °C

With bromine; sodium hydride; potassium carbonate; In chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 29121-25-3
ethyl 2-(3-bromo-4-hydroxyphenyl)acetate

: 1168134-88-0
ethyl 2-(3-bromo-5-chloro-4-(cyclopropylmethoxy)phenyl)-4-methoxybutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuryl dichloride / methanol; dichloromethane / 5 h / Reflux

2.1: potassium carbonate / dimethyl sulfoxide / 4 h / 60 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

3.2: 0.5 h / 0 °C

With sulfuryl dichloride; sodium hydride; potassium carbonate; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;