(+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid

Base Information

Chemical Name:(+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid
CAS No.:86530-42-9
Molecular Formula:Br*C₃₀H₃₄O₂P
Molecular Weight:537.477
Hs Code.:

Synonyms:(+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid

Suppliers and Price of (+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid

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Technology Process of (+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid

There total 3 articles about (+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (+/-)-Diessigsaeure-<(2E)-7-hydroxy-3,7-dimethyl-2-octen-1,6-diyl>ester

: 86530-42-9
(+/-)-Essigsaeure-<(2E)-6-acetoxy-3,7-dimethyl-2,7-octadien-1-yl>triphenylphosphonium-bromid

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / KHCO₃, water / methanol / 168 h / Ambient temperature

2: 1.) PBr₃ / 1.) ether, 0 deg C, 30 min; 2.) ether, benzene, r.t., 48 h

With water; phosphorus tribromide; potassium hydrogencarbonate; In methanol;
DOI:10.1002/hlca.19830660110

Reference yield:

: 78-70-6
3,7-dimethylocta-1,6-dien-3-ol

: 51276-36-9,86530-42-9,86561-89-9,86561-90-2
(6-Acetoxy-3,7-dimethylocta-2,7-dien-1-yl)-triphenylphosphiniumbromid

Guidance literature:: Multi-step reaction with 2 steps

1: (i) methylene blue, O₂, (UV-irradiation), MeOH, (ii) NaBH₄, EtOH, (iii) /BRN= 385737/, Py

2: CHCl₃

In chloroform;