(R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

Base Information

Chemical Name:(R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone
CAS No.:350798-76-4
Molecular Formula:C₁₈H₂₈N₂O₃
Molecular Weight:320.432
Hs Code.:

Synonyms:(R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

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Chemical Property of (R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

Chemical Property:

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Technology Process of (R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

There total 1 articles about (R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1826-67-1
vinyl magnesium bromide

: 146553-06-2,87694-49-3
tert-butyl {(S)-1-[methoxy(methyl)amino]-1-oxopropan-2-yl}carbamate

: 103-67-3
benzyl-methyl-amine

: 350798-76-4
(R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

Guidance literature:: vinyl magnesium bromide; tert-butyl {(S)-1-[methoxy(methyl)amino]-1-oxopropan-2-yl}carbamate; In tetrahydrofuran; at 0 - 20 ℃; for 1.16667h;

benzyl-methyl-amine; In tetrahydrofuran; water; at 20 ℃; for 0.333333h; Further stages.;
DOI:10.1021/jo0057497

Reference yield:

: 350798-76-4
(R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

: [4-(benzyl-methyl-amino)-2-hydroxy-1-methyl-butyl]-carbamic acid tert-butyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; at -20 ℃;
DOI:10.1021/jo0057497

Reference yield:

: 350798-76-4
(R)-2-(N-tert-butoxycarbonyl)amino-5-(N-methyl-N-benzylamino)-3-pentanone

: (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-[2-(benzyl-methyl-amino)-ethyl]-2-tert-butoxycarbonylamino-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / -20 °C

With sodium tetrahydroborate; In methanol;
DOI:10.1021/jo0057497