[4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol

Base Information

• Chemical Name: [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol
• CAS No.: 159929-96-1
• Molecular Formula: C₂₃H₃₅N₃O₂
• Molecular Weight: 385.55

Synonyms:[4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol

Chemical Property of [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol

There total 3 articles about [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C25H35N3O4 (159929-95-0) → [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol (159929-96-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 15h; Heating;

DOI:10.1016/S0040-4039(00)74435-2

Reference yield:

N,N',N''-trimethyldiethylenetriamine (105-84-0) → [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol (159929-96-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / triethylamine / 7 h / 100 °C

2: 90 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; triethylamine;

DOI:10.1016/S0040-4039(00)74435-2

Reference yield:

p-methyloxycarbonylbenzyl chloride (34040-64-7) → [4-({[2-({2-[(4-Hydroxymethyl-benzyl)-methyl-amino]-ethyl}-methyl-amino)-ethyl]-methyl-amino}-methyl)-phenyl]-methanol (159929-96-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / triethylamine / 7 h / 100 °C

2: 90 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; triethylamine;

DOI:10.1016/S0040-4039(00)74435-2

upstream raw materials:

C₂₅H₃₅N₃O₄

N,N',N''-trimethyldiethylenetriamine

p-methyloxycarbonylbenzyl chloride

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