tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate)

Base Information

• Chemical Name: tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate)
• CAS No.: 1609659-43-9
• Molecular Formula: C₃₁H₄₀N₆O₈
• Molecular Weight: 624.694

Synonyms:tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate)

Chemical Property of tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate)

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Technology Process of tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate)

There total 1 articles about tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2-Phenylimidazole (670-96-2) + diethyl 2,3-diazabicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate → diethyl 1-(-5-(2-(1H-imidazol-2-yl)phenyl)cyclopent-2-enyl)hydrazine-1,2-dicarboxylate + tetraethyl 1,1'-2,2'-(2-(1H-imidazol-2-yl)-1,3-phenylene)bis(cyclopent-3-ene-2,1-diyl)bis(hydrazine-1,2-dicarboxylate) (1609659-43-9)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In acetonitrile; at 80 ℃; for 12h; Reagent/catalyst; Solvent; stereoselective reaction; Inert atmosphere;

DOI:10.1055/s-0033-1340221

upstream raw materials:

2-Phenylimidazole

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