phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside
CAS No.:134262-66-1
Molecular Formula:C₁₈H₁₆N₂O₅S₂
Molecular Weight:404.467
Hs Code.:

Synonyms:phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

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Chemical Property of phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

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Technology Process of phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

There total 11 articles about phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125848-19-3,286410-13-7
phenyl-2,4-di-O-acetyl-2,3-dideoxy-1-thio-α-D-threo-hex-2-eno-pyranoside

: 134262-66-1
phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: NaOMe / methanol

2: 86 percent / TBAB / CH₂Cl₂

3: 91 percent / LAH / tetrahydrofuran

4: 1.) MsCl, Et₃N / 2.) DMF

5: 1.) LAH / 1.) THF

With lithium aluminium tetrahydride; tetrabutylammomium bromide; sodium methylate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo951560x

Reference yield:

: 135726-16-8
phenyl 2,3,6-trideoxy-1-thio-α-D-threo-hex-2-enopyranoside

: 134262-66-1
phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MsCl, Et₃N / 2.) DMF

2: 1.) LAH / 1.) THF

With lithium aluminium tetrahydride; methanesulfonyl chloride; triethylamine;
DOI:10.1021/jo951560x

Reference yield:

: 125654-34-4
(2R,3R,6R)-2-Hydroxymethyl-6-phenylsulfanyl-3,6-dihydro-2H-pyran-3-ol

: 134262-66-1
phenyl 2,3,4,6-tetradeoxy-4-<(2,4-dinitrophenyl)dithio>-1-thio-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / TBAB / CH₂Cl₂

2: 91 percent / LAH / tetrahydrofuran

3: 1.) MsCl, Et₃N / 2.) DMF

4: 1.) LAH / 1.) THF

With lithium aluminium tetrahydride; tetrabutylammomium bromide; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo951560x