2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Base Information

Chemical Name:2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester
CAS No.:370097-85-1
Molecular Formula:C₃₈H₄₄O₆
Molecular Weight:596.764
Hs Code.:

Synonyms:2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Suppliers and Price of 2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

There total 7 articles about 2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 370097-70-4
2-(3-(3,4-dimethoxybenzyloxy)-1-propyl)-2-(3-triphenylmethyloxy-1-propyl)malonate diethyl ester

: 370097-85-1
2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Guidance literature:: With water; lithium chloride; In dimethyl sulfoxide; at 140 ℃; for 72h;
DOI:10.1021/jo0101508

Reference yield:

: 596-43-0
bromo-triphenyl-methane

: 370097-85-1
2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 4-dimethylaminopyridine; Et₃N / dimethylformamide / 12 h / 20 °C

2: 47 percent / NaH; Bu₄NI / tetrahydrofuran / 65 °C

3: 13 percent / LiCl; H₂O / dimethylsulfoxide / 72 h / 140 °C

With dmap; water; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; lithium chloride; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo0101508

Reference yield:

: 76504-33-1
((3-bromopropoxy)methanetrityl)tribenzene

: 370097-85-1
2-[3-(3,4-dimethoxy-benzyloxy)-propyl]-5-trityloxy-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / NaH; Bu₄NI / tetrahydrofuran / 65 °C

2: 13 percent / LiCl; H₂O / dimethylsulfoxide / 72 h / 140 °C

With water; tetra-(n-butyl)ammonium iodide; sodium hydride; lithium chloride; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jo0101508