tert-butyl 5-[[3-[(3,4-dimethyl-5-tert-butoxycarbonyl-1H-pyrrol-2-yl)methylidene]-2-oxo-cyclopentylidene]methyl]-3,4-dimethyl-1H-pyrrole-2-carboxylate

Base Information

Chemical Name:tert-butyl 5-[[3-[(3,4-dimethyl-5-tert-butoxycarbonyl-1H-pyrrol-2-yl)methylidene]-2-oxo-cyclopentylidene]methyl]-3,4-dimethyl-1H-pyrrole-2-carboxylate
CAS No.:4914-45-8
Molecular Formula:C₂₂H₂₅ClN₂O₅
Molecular Weight:432.904
Hs Code.:
Mol file:4914-45-8.mol

tert-butyl 5-[[3-[(3,4-dimethyl-5-tert-butoxycarbonyl-1H-pyrrol-2-yl)methylidene]-2-oxo-cyclopentylidene]methyl]-3,4-dimethyl-1H-pyrrole-2-carboxylate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 5-[[3-[(3,4-dimethyl-5-tert-butoxycarbonyl-1H-pyrrol-2-yl)methylidene]-2-oxo-cyclopentylidene]methyl]-3,4-dimethyl-1H-pyrrole-2-carboxylate

Chemical Property:

Boiling Point:691.1°Cat760mmHg
Flash Point:371.7°C
Density:1.184g/cm³

Purity/Quality:

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Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl 5-[[3-[(3,4-dimethyl-5-tert-butoxycarbonyl-1H-pyrrol-2-yl)methylidene]-2-oxo-cyclopentylidene]methyl]-3,4-dimethyl-1H-pyrrole-2-carboxylate

There total 3 articles about tert-butyl 5-[[3-[(3,4-dimethyl-5-tert-butoxycarbonyl-1H-pyrrol-2-yl)methylidene]-2-oxo-cyclopentylidene]methyl]-3,4-dimethyl-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2650-70-6
L-N-Carbobenzoxy-glutaminsaeure-α-(2-hydroxyethyl)-amid-γ-benzylester

: 4914-45-8
L-N-Carbobenzoxy-glutaminsaeure-α-(2-chloraethyl)-amid-γ-benzylester

Guidance literature:: With pyridine; thionyl chloride; In chloroform;
DOI:10.1021/jm00319a022

Reference yield:

: 5680-86-4
N-benzyloxycarbonyl-5-O-benzyl-L-glutamic acid

: 4914-45-8
L-N-Carbobenzoxy-glutaminsaeure-α-(2-chloraethyl)-amid-γ-benzylester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / Ambient temperature

2: ethyl acetate / Ambient temperature

3: SOCl₂, Py / CHCl₃

With pyridine; thionyl chloride; triethylamine; In chloroform; ethyl acetate;
DOI:10.1021/jm00319a022

Reference yield:

: 4821-83-4
L-N-Carbobenzoxy-glutaminsaeure-α-cyanmethylester-γ-benzylester

: 4914-45-8
L-N-Carbobenzoxy-glutaminsaeure-α-(2-chloraethyl)-amid-γ-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / Ambient temperature

2: SOCl₂, Py / CHCl₃

With pyridine; thionyl chloride; In chloroform; ethyl acetate;
DOI:10.1021/jm00319a022