C₁₇H₈ClF₄NO

Base Information

Chemical Name:C₁₇H₈ClF₄NO
CAS No.:1416806-10-4
Molecular Formula:C₁₇H₈ClF₄NO
Molecular Weight:353.703
Hs Code.:

C<sub>17</sub>H<sub>8</sub>ClF<sub>4</sub>NO

Synonyms:C₁₇H₈ClF₄NO

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Chemical Property of C₁₇H₈ClF₄NO

Chemical Property:

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Technology Process of C₁₇H₈ClF₄NO

There total 9 articles about C₁₇H₈ClF₄NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 348-57-2
2,4-difluorobromobenzene

: 1416806-09-1
C₁₃H₁₀ClF₂NO₂

: 1416806-10-4
C₁₇H₈ClF₄NO

Guidance literature:: 2,4-difluorobromobenzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; Inert atmosphere;

C₁₃H₁₀ClF₂NO₂; In diethyl ether; hexane; at -78 - 20 ℃; for 1.25h; Inert atmosphere;

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1416806-10-4
C₁₇H₈ClF₄NO

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium cyanide / water; methanol / 20 - 70 °C

2.1: 6 h / 120 °C / Inert atmosphere

3.1: ammonia / dichloromethane; water / 0.5 h / -25 °C / Inert atmosphere

4.1: copper(ll) sulfate pentahydrate / ethanol; water / 0.5 h / Inert atmosphere; Reflux

5.1: trifluoroacetic acid / ethanol / Inert atmosphere; Reflux

6.1: trifluoroacetic acid / dichloromethane / 3 h / Inert atmosphere; Reflux

7.1: sodium nitrite; hydrogen bromide / water / 1.25 h / 0 °C

8.1: bronze powder / dimethyl sulfoxide / 16 h / Inert atmosphere

9.1: n-butyllithium / hexane; diethyl ether / -78 °C / Inert atmosphere

9.2: 1.25 h / -78 - 20 °C / Inert atmosphere

With sodium cyanide; bronze powder; n-butyllithium; copper(ll) sulfate pentahydrate; ammonia; hydrogen bromide; trifluoroacetic acid; sodium nitrite; trifluoroacetic acid; In methanol; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 135737-05-2
(4-Chloro-phenyl)-(cyanomethyl-methyl-amino)-acetonitrile

: 1416806-10-4
C₁₇H₈ClF₄NO

Guidance literature:: Multi-step reaction with 8 steps

1.1: 6 h / 120 °C / Inert atmosphere

2.1: ammonia / dichloromethane; water / 0.5 h / -25 °C / Inert atmosphere

3.1: copper(ll) sulfate pentahydrate / ethanol; water / 0.5 h / Inert atmosphere; Reflux

4.1: trifluoroacetic acid / ethanol / Inert atmosphere; Reflux

5.1: trifluoroacetic acid / dichloromethane / 3 h / Inert atmosphere; Reflux

6.1: sodium nitrite; hydrogen bromide / water / 1.25 h / 0 °C

7.1: bronze powder / dimethyl sulfoxide / 16 h / Inert atmosphere

8.1: n-butyllithium / hexane; diethyl ether / -78 °C / Inert atmosphere

8.2: 1.25 h / -78 - 20 °C / Inert atmosphere

With bronze powder; n-butyllithium; copper(ll) sulfate pentahydrate; ammonia; hydrogen bromide; trifluoroacetic acid; sodium nitrite; trifluoroacetic acid; In diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide;