N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

Base Information

Chemical Name:N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate
CAS No.:1393818-71-7
Molecular Formula:C₈H₁₇N*C₂₅H₂₂NO₃PS
Molecular Weight:574.724
Hs Code.:

Synonyms:N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

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Chemical Property of N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

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Technology Process of N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

There total 6 articles about N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-89-4
piperidine

: 1393818-67-1
C₂₈H₂₈NO₃PS

: 1393818-71-7
N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

Guidance literature:: In chloroform-d1; at 68 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.06.112

Reference yield:

: 1393818-82-0
propyl 2-amino-5-methylbenzenesulfonate

: 1393818-71-7
N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrafluoroboric acid / water / 0.25 h / 0 °C

1.2: 0.33 h / 0 °C

2.1: sodium azide / water / 2 h / 0 - 25 °C

3.1: toluene / 4 h / 25 °C / Inert atmosphere

4.1: chloroform-d1 / 72 h / 68 °C / Inert atmosphere

With tetrafluoroboric acid; sodium azide; In chloroform-d1; water; toluene; 3.1: Staudinger reaction;
DOI:10.1016/j.tetlet.2012.06.112

Reference yield:

: BF₄^(1-)*C₁₀H₁₃N₂O₃S⁽¹⁺⁾

: 1393818-71-7
N-propylpiperidinium 2-((triphenylphosphoranylidene)amino)-5-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / water / 2 h / 0 - 25 °C

2: toluene / 4 h / 25 °C / Inert atmosphere

3: chloroform-d1 / 72 h / 68 °C / Inert atmosphere

With sodium azide; In chloroform-d1; water; toluene; 2: Staudinger reaction;
DOI:10.1016/j.tetlet.2012.06.112