propyl 2-amino-5-methylbenzenesulfonate

Base Information

Chemical Name:propyl 2-amino-5-methylbenzenesulfonate
CAS No.:1393818-82-0
Molecular Formula:C₁₀H₁₅NO₃S
Molecular Weight:229.3
Hs Code.:

Synonyms:propyl 2-amino-5-methylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propyl 2-amino-5-methylbenzenesulfonate

Chemical Property:

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Technology Process of propyl 2-amino-5-methylbenzenesulfonate

There total 2 articles about propyl 2-amino-5-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 71-23-8
propan-1-ol

: 2-amino-5-methylbenzenesulfonyl chloride

: 1393818-82-0
propyl 2-amino-5-methylbenzenesulfonate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; at 0 - 25 ℃; for 16.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.06.112

Reference yield:

: 71-23-8
propan-1-ol

: 88-44-8
2-Amino-5-methylbenzenesulfonic acid

: 1393818-82-0
propyl 2-amino-5-methylbenzenesulfonate

Guidance literature:: 2-Amino-5-methylbenzenesulfonic acid; With chlorosulfonic acid; at 0 - 80 ℃; for 3h; Inert atmosphere;

propan-1-ol; With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; at 25 ℃; for 16h; Inert atmosphere;
DOI:10.1021/om501262r

Reference yield: 25.0%

: 1393818-82-0
propyl 2-amino-5-methylbenzenesulfonate

: 1393818-84-2
n-propyl 2-azido-5-methylbenzenesulfonate

Guidance literature:: propyl 2-amino-5-methylbenzenesulfonate; With tetrafluoroboric acid; In ethanol; water; at 0 ℃; for 0.333333h; Inert atmosphere;

With sodium nitrite; In ethanol; water; at 0 ℃; for 0.333333h; Inert atmosphere;

With sodium azide; In water; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/om501262r