sodium 2-methoxy-5-methylbenzene sulphinate

Base Information

Chemical Name:sodium 2-methoxy-5-methylbenzene sulphinate
CAS No.:82635-16-3
Molecular Formula:C₈H₉O₃S*Na
Molecular Weight:208.213
Hs Code.:

Synonyms:sodium 2-methoxy-5-methylbenzene sulphinate

Suppliers and Price of sodium 2-methoxy-5-methylbenzene sulphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of sodium 2-methoxy-5-methylbenzene sulphinate

Chemical Property:

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Technology Process of sodium 2-methoxy-5-methylbenzene sulphinate

There total 2 articles about sodium 2-methoxy-5-methylbenzene sulphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 88040-86-2
2-methoxy-5-methylbenzene sulfonyl chloride

: 82635-16-3
sodium 2-methoxy-5-methylbenzene sulphinate

Guidance literature:: With sodium hydrogencarbonate; sodium sulfite; In water; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jacs.0c03239

Reference yield:

: 104-93-8
p-methylanizole

: 82635-16-3
sodium 2-methoxy-5-methylbenzene sulphinate

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 0 - 20 °C / Schlenk technique; Inert atmosphere

2: sodium hydrogencarbonate; sodium sulfite / water / 4 h / 80 °C / Inert atmosphere

With chlorosulfonic acid; sodium hydrogencarbonate; sodium sulfite; In water;
DOI:10.1021/jacs.0c03239

Reference yield: 99.0%

: 52017-21-7
(3-bromo-3-methyl-n-butyl)benzene

: 82635-16-3
sodium 2-methoxy-5-methylbenzene sulphinate

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: (E)-2-((5,5-dimethyl-7-phenylhept-2-en-1-yl)sulfonyl)-1-methoxy-4-methylbenzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; N,N-dimethyl acetamide; at 20 ℃; for 48h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/jacs.0c03239