(Z)-2-fluoro-2-trifluoromethylethenyl tosylate

Base Information

Chemical Name:(Z)-2-fluoro-2-trifluoromethylethenyl tosylate
CAS No.:212619-47-1
Molecular Formula:C₁₀H₈F₄O₃S
Molecular Weight:284.231
Hs Code.:

Synonyms:(Z)-2-fluoro-2-trifluoromethylethenyl tosylate

Suppliers and Price of (Z)-2-fluoro-2-trifluoromethylethenyl tosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-fluoro-2-trifluoromethylethenyl tosylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (Z)-2-fluoro-2-trifluoromethylethenyl tosylate

There total 2 articles about (Z)-2-fluoro-2-trifluoromethylethenyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 565-42-4
2,2,3,3,3-pentafluoro-1-propyl 4-toluenesulfonate

: 212619-47-1
(Z)-2-fluoro-2-trifluoromethylethenyl tosylate

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 212619-47-1
(Z)-2-fluoro-2-trifluoromethylethenyl tosylate

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / CH₂Cl₂ / 3 h / Ambient temperature

2: 67 percent / n-BuLi, 1,3-dimethylperhydropyrimidin-2-one / tetrahydrofuran; hexane / 0.17 h / -78 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane;

Reference yield: 80.0%

: 212619-47-1
(Z)-2-fluoro-2-trifluoromethylethenyl tosylate

: 98-80-6
phenylboronic acid

: 102816-92-2
(Z)-<2,3,3,3-Tetrafluoro-1-propenyl>benzene

Guidance literature:: With potassium phosphate; palladium diacetate; tricyclohexylphosphine; In 1,4-dioxane; water; at 100 ℃; for 4h; Reagent/catalyst; Solvent; Temperature; stereoselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1002/bkcs.11419