(E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

Base Information

Chemical Name:(E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester
CAS No.:142801-54-5
Molecular Formula:C₂₉H₂₆F₅NO₅
Molecular Weight:563.521
Hs Code.:

Synonyms:(E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

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Chemical Property of (E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

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Technology Process of (E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

There total 4 articles about (E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82689-15-4
O-benzyl-N-(tert-butoxycarbonyl)-L-tyrosinal

: 142801-54-5
(E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: LiOH / methanol; H₂O

3: DCC / CH₂Cl₂

With lithium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1021/ja00042a053

Reference yield:

: 126410-45-5
tert-butyl (S)-{3-[4-(benzyloxy)phenyl]-1-[methoxy(methyl)amino]-1-oxo-propan-2-yl}carbamate

: 142801-54-5
(E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / tetrahydrofuran

3: LiOH / methanol; H₂O

4: DCC / CH₂Cl₂

With lithium hydroxide; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja00042a053

Reference yield:

: (E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid ethyl ester

: 142801-54-5
(E)-(S)-5-(4-Benzyloxy-phenyl)-4-tert-butoxycarbonylamino-pent-2-enoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiOH / methanol; H₂O

2: DCC / CH₂Cl₂

With lithium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1021/ja00042a053