N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

Base Information

Chemical Name:N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide
CAS No.:1581304-48-4
Molecular Formula:C₁₇H₁₁Cl₂N₃O₃
Molecular Weight:376.199
Hs Code.:

Synonyms:N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

Suppliers and Price of N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

There total 2 articles about N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1581304-46-2
3,5-dichloro-4-((6-chloropyridazin-3-yl)oxy)aniline

: 93-97-0
benzoic acid anhydride

: 1581304-48-4
N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

Guidance literature:: 3,5-dichloro-4-((6-chloropyridazin-3-yl)oxy)aniline; benzoic acid anhydride; With acetic acid; at 100 ℃; for 0.583333h; Large scale;

With sodium acetate; at 110 ℃; for 14.5h; Reagent/catalyst; Solvent; Temperature; Large scale;

Reference yield:

: 5930-28-9
4-amino-2,6-dichlorophenol

: 1581304-48-4
N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl acetamide / 19 h / 70 - 110 °C / Large scale

2.1: acetic acid / 0.58 h / 100 °C / Large scale

2.2: 14.5 h / 110 °C / Large scale

With caesium carbonate; acetic acid; In N,N-dimethyl acetamide;

Reference yield:

: 1581304-48-4
N-(3,5-dichloro-4-((6-oxo-1,6-dihydropyridazin-3-yl)oxy)phenyl)benzamide

: 920509-32-6
2-[3,5-dichloro-4-[[1,6-dihydro-5-(1-methylethyl)-6-oxo-3-pyridazinyl]oxy]phenyl]-2,3,4,5-tetrahydro-3,5-dioxo-1,2,4-triazine-6-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium chloride / tetrahydrofuran / 5.83 h / 35 - 45 °C / Large scale

2.1: potassium hydroxide; water / 11 h / 85 °C / Large scale

3.1: hydrogenchloride; sodium nitrite; acetic acid / water / 0.33 h / 5 - 10 °C / Large scale

3.2: 0.68 h / 10 °C / Large scale

4.1: potassium acetate / N,N-dimethyl acetamide / 2 h / 120 °C / Large scale

With hydrogenchloride; water; potassium acetate; acetic acid; lithium chloride; potassium hydroxide; sodium nitrite; In tetrahydrofuran; N,N-dimethyl acetamide; water;