Technology Process of C23H31FN4O3
There total 7 articles about C23H31FN4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 120h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 130 °C / microwave irradiation
2: hydrogenchloride; hydrogen / 5%-palladium/activated carbon / water; methanol / 50 °C / 37503.8 Torr
3: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 120 h
With
hydrogenchloride; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
copper(l) iodide; 5%-palladium/activated carbon; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane / 2 h
2: acetic anhydride; potassium acetate; acetic acid; isopentyl nitrite / toluene / 2 h / Reflux
3: potassium carbonate; methanol / 0.08 h / Reflux
4: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 130 °C / microwave irradiation
5: hydrogenchloride; hydrogen / 5%-palladium/activated carbon / water; methanol / 50 °C / 37503.8 Torr
6: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 120 h
With
hydrogenchloride; methanol; hydrogen; potassium acetate; acetic anhydride; potassium carbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; isopentyl nitrite;
copper(l) iodide; 5%-palladium/activated carbon; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;