7-amino-1-benzyloxycarbonylaminooctane

Base Information

Chemical Name:7-amino-1-benzyloxycarbonylaminooctane
CAS No.:207980-88-9
Molecular Formula:C₁₆H₂₆N₂O₂
Molecular Weight:278.395
Hs Code.:

Synonyms:7-amino-1-benzyloxycarbonylaminooctane

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Chemical Property of 7-amino-1-benzyloxycarbonylaminooctane

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Technology Process of 7-amino-1-benzyloxycarbonylaminooctane

There total 12 articles about 7-amino-1-benzyloxycarbonylaminooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 207980-87-8
1-benzyloxycarbonylamino-7-tert-butyloxycarbonylaminooctane

: 207980-88-9
7-amino-1-benzyloxycarbonylaminooctane

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 1h;
DOI:10.1016/S0968-0896(97)10030-X

Reference yield:

: 62992-46-5
1-(tetrahydropyranyloxy)-4-pentyn

: 207980-88-9
7-amino-1-benzyloxycarbonylaminooctane

Guidance literature:: Multi-step reaction with 11 steps

1: 1.) n-butyllithium, 2.) hexamethylphosphoramide / 1.) THF, hexane, 2 h, 2.) THF, hexane, -50 deg C -> room temperature

2: 92 percent / triethylamine / CH₂Cl₂ / 0.25 h

3: 67 percent / NaN₃ / dimethylsulfoxide

4: 96 percent / hydrogen / PtO₂ / ethanol / 6 h / 2068.6 Torr

5: 94 percent / dimethylformamide / 0.5 h

6: 86 percent / pyridinium-p-toluene sulfonate / aq. ethanol / 5 h / 53 - 58 °C

7: 87 percent / triethylamine / CH₂Cl₂ / 0.25 h

8: 89 percent / NaN₃ / dimethylsulfoxide

9: 98 percent / hydrogen / PtO₂ / ethanol / 6 h / 2068.6 Torr

10: 85 percent / CHCl₃ / Ambient temperature

11: 91 percent / trifluoroacetic acid / 1 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium azide; hydrogen; pyridinium p-toluenesulfonate; triethylamine; trifluoroacetic acid; platinum(IV) oxide; In ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(97)10030-X

Reference yield:

: 207980-79-8
1-(2-tetrahydropyranyloxy)-7-aminooctane

: 207980-88-9
7-amino-1-benzyloxycarbonylaminooctane

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / dimethylformamide / 0.5 h

2: 86 percent / pyridinium-p-toluene sulfonate / aq. ethanol / 5 h / 53 - 58 °C

3: 87 percent / triethylamine / CH₂Cl₂ / 0.25 h

4: 89 percent / NaN₃ / dimethylsulfoxide

5: 98 percent / hydrogen / PtO₂ / ethanol / 6 h / 2068.6 Torr

6: 85 percent / CHCl₃ / Ambient temperature

7: 91 percent / trifluoroacetic acid / 1 h / 0 °C

With sodium azide; hydrogen; pyridinium p-toluenesulfonate; triethylamine; trifluoroacetic acid; platinum(IV) oxide; In ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(97)10030-X