4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane

Base Information

Chemical Name:4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane
CAS No.:959839-23-7
Molecular Formula:C₁₉H₂₃FN₄O₂
Molecular Weight:358.416
Hs Code.:

Synonyms:4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane

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Chemical Property of 4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane

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Technology Process of 4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane

There total 2 articles about 4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1154868-49-1
C₂₄H₃₁FN₄O₄

: 959839-23-7
4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane

Guidance literature:: C₂₄H₃₁FN₄O₄; With hydrogenchloride; ethanol; at 20 ℃; for 1h;

With ammonia; water; pH=9;

Reference yield:

: 959841-43-1
5-[(5-ethyl-6-oxo-1,6-dihydropyridazin-3-yl)methyl]-2-fluorobenzoic Acid

: 959839-23-7
4-{5-[(5-ethyl-6-oxo-1,6-dihydro-pyridazin-3-yl)methyl]-2-fluoro-benzoyl}-1,4-diazepane

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 20 °C

2.1: hydrogenchloride; ethanol / 1 h / 20 °C

2.2: pH 9

With hydrogenchloride; ethanol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide;