N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide

Base Information

Chemical Name:N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide
CAS No.:1443013-27-1
Molecular Formula:C₄₃H₇₂N₆O₁₄S₂
Molecular Weight:961.208
Hs Code.:

Synonyms:N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide

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Chemical Property of N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide

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Technology Process of N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide

There total 2 articles about N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1443013-26-0
N-[(20-aminohexaethylene glycolyl)-1H-[1,2,3]-triazole-4-ylmethyl]-11-thioacetyl-undecanoic acid amide

: 96345-79-8
[p-isothiocyanato]-phenyl α-D-mannopyranoside

: 1443013-27-1
N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1039/c3ob40386f

Reference yield:

: 957486-82-7
O-(2-aminoethyl)-O′-(2-azidoethyl)pentaethylene glycol

: 1043884-36-1
C₁₆H₂₇NO₂S

: 1443013-27-1
N-{20-[p-(α-D-mannopyranosyloxy)-phenylthioureidohexaethyleneglycolyl]-1H-[1,2,3]-triazole-4-yl-methyl}-11-thioacetyl-undecanoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide / acetonitrile / 24 h / 45 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3ob40386f