tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate
CAS No.:1259323-14-2
Molecular Formula:C₂₃H₂₉N₃O₃S₂
Molecular Weight:459.634
Hs Code.:

Synonyms:tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

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Technology Process of tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

There total 4 articles about tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62056-52-4
butyl 3-(trichlorovinyl)-4,5-dihydroisoxazole-5-carboxylate

: 1259323-07-3
amino[({2-[1-(tert-butoxycarbonyl)piperidin-4-yl]-1,3-thiazol-4-yl}methyl)sulphanyl]methaniminium iodide

: 1259323-14-2
tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In water; toluene; at 20 ℃; for 2h;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1259323-14-2
tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chloro-succinimide / 1,2-dimethoxyethane / 75 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium hydroxide; tetrabutylammomium bromide / toluene; water / 2 h / 20 °C

With N-chloro-succinimide; tetrabutylammomium bromide; sodium hydroxide; In 1,2-dimethoxyethane; water; toluene;

Reference yield:

: 864068-79-1
tert- butyl 4-(4-(hydroxymethyl)thiazol-2-yl)piperidine-1-carboxylate

: 1259323-14-2
tert-butyl 4-[4-({[5-phenyl-4,5-dihydro-1,2-oxazol-3-yl]sulphanyl}methyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 0.5 h

2: ethanol / 3 h / 20 °C

3: sodium hydroxide; tetrabutylammomium bromide / toluene; water / 2 h / 20 °C

With 1H-imidazole; tetrabutylammomium bromide; iodine; triphenylphosphine; sodium hydroxide; In ethanol; dichloromethane; water; toluene;