nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate)

Base Information

• Chemical Name: nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate)
• CAS No.: 103992-66-1
• Molecular Formula: C₂₀H₁₇N₃NiO₃
• Molecular Weight: 406.063
• Mol file: 103992-66-1.mol

Synonyms:nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate)

Chemical Property of nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate)

Chemical Property:

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Technology Process of nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate)

There total 1 articles about nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

salicylaldehyde-oxime (94-67-7) + nickel dichloride (83864-14-6) + 2-hydroxybenzaldehyde phenylhydrazone (614-65-3) → nickel (salicylaldehyde phenylhydrazonate)(salicylaldoximate) (103992-66-1)

Guidance literature:

With NaOH; In ethanol; water; acetone; dropwise addn. of aq. soln. of NiCl2 to mixt. of NaOH and ligands in mixt. of acetone/EtOH/water 2:1:1 (stirring), pptn.; filtration off, washing (EtOH), drying (vac.); elem. anal.;

DOI:10.1016/0584-8539(86)80091-5

upstream raw materials:

salicylaldehyde-oxime

nickel dichloride

2-hydroxybenzaldehyde phenylhydrazone