Nickel chloride-Ni63

Base Information

• Chemical Name: Nickel chloride-Ni63
• CAS No.: 83864-14-6
• Molecular Formula: Cl₂Ni
• Molecular Weight: 129.596
• Mol file: 83864-14-6.mol

Synonyms:Nickel chloride-Ni63

Chemical Property of Nickel chloride-Ni63

Chemical Property:

• PSA: 0.00000
• LogP: -5.99200

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nickel chloride-Ni63

There total 314 articles about Nickel chloride-Ni63 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

[((C6H5)3P)3NiCl]2 → bis(triphenylphosphine)nickel(II) chloride (14264-16-5,53996-95-5,62075-39-2,39716-73-9) + nickel (7440-02-0) + nickel dichloride (83864-14-6)

Guidance literature:

In neat (no solvent); byproducts: triphenylphosphine; Ar-atmosphere; 140-180°C, 1 h; extn. (ether, CH2Cl2, H2O), evapn. of extract;

DOI:10.1016/S0020-1693(00)90496-1

Reference yield: 50.0%

L-(S)-Ni(OC(O)CH(CH(CO2C2H5)2)NC(C6H5)C6H4NC(O)CH(CH2)3NCH2C6H5) + diethyl malonate (105-53-3) → L-Aspartic acid (56-84-8,25608-40-6,27881-03-4,32505-46-7,52526-39-3) + (S)-N-(2-benzoylphenyl)-1-benzylpyrrolidine-2-carboxamide (96293-17-3,105024-93-9,105112-33-2) + nickel dichloride (83864-14-6)

Guidance literature:

In hydrogenchloride; boiling for 1 h;;

DOI:10.1039/c39880001336

Reference yield:

nickel silicate → tetrachlorosilane (10026-04-7,53609-55-5) + nickel dichloride (83864-14-6)

Guidance literature:

With chlorine; In neat (no solvent); at 15 - 450°C; acceleration by moisture;;

upstream raw materials:

nickel

hydrogenchloride

thiophosgene

tetracarbonyl nickel

Downstream raw materials:

((C₆H₅CHNC₂H₄)2NCS₂)Ni(S₂CNH₂)

manganese(ll) chloride

Refernces

• 1、 Mohamed, M. A.,Halawy, S. A.. "Non-isothermal kinetic and thermodynamic study for the dehydration of copper(II) chloride dihydrate and nickel chloride hexahydrate". . p. 147 - 160. Retrieved 1994.
• 2、 Yang, Baojun,Hu, Hanmei,Wu, Yucheng,Luo, Tao,Yang, Xiaogang,Qian, Yitai. "A co-reduction-silicification route to δ-Ni2Si nanowire". . p. 326 - 327. Retrieved 2005.
• 3、 Lee, M. F.. "". . p. 877 - 878. Retrieved 1958.
• 4、 Meyer, Gerd,Nockemann, Peter. "Reactivity of ammonium chloride/mercuric chloride mixtures with monel containers. The new compounds (NH4)2(NH3)x[Ni(NH3) 2Cl4] and (NH4)5Cl2[CuCl2] [CuCl4]". . p. 254 - 259. Retrieved 2001.
• 5、 Beaver, W. D.,Trevorrov, L. E.,Estill, W. B.,Yates, P. C.,Moore, T. E.. "". . p. 4556 - 4560. Retrieved 1953.
• 6、 Johnson, J. W.,Cubicciotti, D.,Kelley, C. M.. "". . p. 1107 - 1109. Retrieved 1958.
• 7、 Kapoor, Ramesh,Kataria, Ashok,Pathak, Anuradha,Venugopalan, Paloth,Hundal, Geeta,Kapoor, Pratibha. "X-ray diffraction, spectral and magnetic studies of the nickel(II) thiocyanate complexes with tridentate 2,6-dithiocarboxamidopyridine SNS and 2,6-dicarboxamidopyridine ONO ligands: Influence of donor atoms on the coordination geometry of nickel". . p. 1221 - 1231. Retrieved 2005.
• 8、 Hougen, J. T.,Leroi, G. E.,James, T. C.. "". . p. 1670 - 1677. Retrieved 1961.
• 9、 Liu, Bo,Liu, Xiaolong,Chen, Chao,Chen, Congyan,Chen, Wanzhi. "Carbene transfer reactivities of nickel(II)-N-heterocyclic carbene complexes and their applications in the synthesis of metal-NHC complexes". . p. 282 - 288. Retrieved 2012.
• 10、 Liu, Yongjun,Xiao, Shuhuan,Qi, Yan,Du, Feng. "Reductive Homocoupling of Organohalides Using Nickel(II) Chloride and Samarium Metal". supporting information. p. 673 - 678. Retrieved 2017/03/22.