2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

Base Information

Chemical Name:2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile
CAS No.:324817-77-8
Molecular Formula:C₂₂H₁₆N₂O₂
Molecular Weight:340.381
Hs Code.:

Synonyms:2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

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Chemical Property of 2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

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Technology Process of 2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

There total 1 articles about 2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 324817-75-6
1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-ol

: 590-17-0
cyanomethyl bromide

: 324817-77-8
2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 1.5h;

Reference yield:

: 324817-77-8
2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

: 324817-03-0
[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]ethanamine

Guidance literature:: 2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile; With dimethylsulfide borane complex; In tetrahydrofuran; at 75 ℃; for 3h;

With hydrogenchloride; In methanol; dichloromethane; water; for 2h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 324817-77-8
2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile

: 324817-05-2
N-isopropyl-N-{2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]ethyl}amine

: 324817-03-0
[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]ethanamine

Guidance literature:: 2-[(1-phenyl-1,2-dihydro[1,4]oxazino[2,3,4-jk]carbazol-7-yl)oxy]acetonitrile; With dimethylsulfide borane complex; In tetrahydrofuran; at 80 ℃; for 1.75h;

With hydrogenchloride; In water; acetone; at 65 - 70 ℃; for 0.25h;

With sodium hydrogencarbonate; In dichloromethane; water;