(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂)

Base Information

• Chemical Name: (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂)
• CAS No.: 410527-33-2
• Molecular Formula: C₂₉H₄₁CuN₂O₂
• Molecular Weight: 513.203
• Mol file: 410527-33-2.mol

Synonyms:(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂)

Chemical Property of (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂)

There total 9 articles about (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile) (410527-15-0) + oxygen (80937-33-3) → (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O2) (410527-33-2)

Guidance literature:

In acetone; (N2); dissolving copper complex in acetone, cooling to 193 K, bubbling O2 for 30 min; storage at 193 K overnight, sepn., washing with pentane at 193 K, dryingin vac. at 193 K;

DOI:10.1021/ja045678j

Reference yield:

(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile) (410527-15-0) → (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O2) (410527-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: tetrahydrofuran

In tetrahydrofuran;

DOI:10.1021/ja045678j

Reference yield:

(C6H3(CH(CH3)2)2NCCH3)2CHCuNCC6H4CN + oxygen (80937-33-3) → (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O2) (410527-33-2)

Guidance literature:

In tetrahydrofuran; (N2); react. of copper complex with O2 in THF at 203 K; UV detection; Kinetics;

DOI:10.1021/ja045678j

upstream raw materials:

(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile)

oxygen

(C₆H₃(CH(CH₃)2)2NCCH₃)2CHCu(CH₃CH₂CN)

(C₆H₃(CH(CH₃)2)2NCCH₃)2CHCu(NCC₆H₅)

Downstream raw materials:

[(N(C₆H₃(CH(CH₃)2)2)C(CH₃)CHC(CH₃)N(C₆H₃(CH(CH₃)2)2))Cu(O)2Cu(N(C₆H₃(CH₃)2)C(CH₃)CHC(CH₃)N(C₆H₃(CH₃)2))]

[(CH(C(CH3)NC6H3(CH(CH3)2)2)2bis(μ-oxo)copper(III)nickel(III)(phenyltris((tert-butylthio)methyl)borate)]