6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

Base Information

Chemical Name:6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide
CAS No.:90957-06-5
Molecular Formula:C₂₆H₃₄N₄O₆S₂*HI
Molecular Weight:690.624
Hs Code.:

Synonyms:6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

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Chemical Property of 6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

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Technology Process of 6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

There total 4 articles about 6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 90957-03-2
6-{2-[3-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid

: 74-88-4
methyl iodide

: 90957-06-5
6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

Guidance literature:: In methanol; acetone; for 18h; Ambient temperature;

Reference yield:

: 90957-00-9
N-(Nα-Tosyl-4-cyanphenylalanyl)glycyl-ε-aminocapronsaeure

: 90957-06-5
6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂S (gas) / pyridine; triethylamine / Ambient temperature

2: 91 percent / acetone; methanol / 18 h / Ambient temperature

With hydrogen sulfide; In pyridine; methanol; triethylamine; acetone;

Reference yield:

: 90282-17-0
N-(N_α-Tosyl-4-cyanphenylalanyl)glycin-(4-nitrophenylester)

: 90957-06-5
6-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-hexanoic acid; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / 1M NaOH / pyridine; H₂O / 2 h / Ambient temperature

2: 94 percent / H₂S (gas) / pyridine; triethylamine / Ambient temperature

3: 91 percent / acetone; methanol / 18 h / Ambient temperature

With sodium hydroxide; hydrogen sulfide; In pyridine; methanol; water; triethylamine; acetone;