Technology Process of 1,4,5,8-tetrahydronaphthalene-2,3-diyldimethanol
There total 4 articles about 1,4,5,8-tetrahydronaphthalene-2,3-diyldimethanol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
1.) 0 deg C, 2.) ambient temp., 4h;
DOI:10.1021/jo00150a030
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / benzene / 4 h / 40 - 50 °C
2: 85 percent / LiAlH4 / diethyl ether / 1.) 0 deg C, 2.) ambient temp., 4h
With
lithium aluminium tetrahydride;
In
diethyl ether; benzene;
DOI:10.1021/jo00150a030
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) sodium iodide, chlorotrimethylsilane, 2.) Zn-Cu couple / 1.) ether, 25 deg C, 1h, 2.) ether, 2h
2: 94 percent / benzene / 4 h / 40 - 50 °C
3: 85 percent / LiAlH4 / diethyl ether / 1.) 0 deg C, 2.) ambient temp., 4h
With
lithium aluminium tetrahydride; chloro-trimethyl-silane; copper; sodium iodide; zinc;
In
diethyl ether; benzene;
DOI:10.1021/jo00150a030
