2,2,2-trichloroethyl cyclohex-2-enylcarbamate

Base Information

Chemical Name:2,2,2-trichloroethyl cyclohex-2-enylcarbamate
CAS No.:871565-04-7
Molecular Formula:C₉H₁₂Cl₃NO₂
Molecular Weight:272.559
Hs Code.:

Synonyms:2,2,2-trichloroethyl cyclohex-2-enylcarbamate

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Chemical Property of 2,2,2-trichloroethyl cyclohex-2-enylcarbamate

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Technology Process of 2,2,2-trichloroethyl cyclohex-2-enylcarbamate

There total 3 articles about 2,2,2-trichloroethyl cyclohex-2-enylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 871565-06-9
2,2,2-trichloroethyl octa-1,7-dien-3-ylcarbamate

: 871565-04-7
2,2,2-trichloroethyl cyclohex-2-enylcarbamate

Guidance literature:: With Grubbs catalyst first generation; In toluene; at 60 ℃; for 2h;
DOI:10.1021/ja055806j

Reference yield: 44.0%

: 2,2,2-trichloroethyl ((4-cyanobenzoyl)oxy)carbamate

: 110-83-8
cyclohexene

: 871565-04-7
2,2,2-trichloroethyl cyclohex-2-enylcarbamate

Guidance literature:: With Ir(2-(2-pyridinyl)-3,5-difluorophenyl)₂(2-(2-pyridinyl)phenyl); water; copper(II) dipivaloate; magnesium trimethylacetate; In acetonitrile; at 20 ℃; for 24h; Irradiation; Inert atmosphere;
DOI:10.1039/d0sc05952h

Reference yield:

: 71663-71-3
3-amino-1,7-octadiene

: 871565-04-7
2,2,2-trichloroethyl cyclohex-2-enylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

2: 87 percent / (Cy₃P)2Cl₂Ru=CHPh / toluene / 2 h / 60 °C

With Grubbs catalyst first generation; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ja055806j