3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

Base Information

Chemical Name:3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride
CAS No.:1285575-37-2
Molecular Formula:C₁₃H₁₇ClO₄S
Molecular Weight:304.795
Hs Code.:

Synonyms:3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

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Chemical Property of 3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

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Technology Process of 3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

There total 7 articles about 3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285575-36-1
3-t-butyl-4-methoxy-5-methylsulfonyl benzoic acid

: 1285575-37-2
3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 60 ℃; for 16h;

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1285575-37-2
3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanesulfonic acid / 16 h / 70 °C

1.2: 3 h / 50 °C

2.1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 0.25 h / 20 °C

3.1: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 3 h / 20 °C

6.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 5 h / 20 °C

7.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

With N-iodo-succinimide; thionyl chloride; methanesulfonic acid; lithium hydroxide monohydrate; trifluorormethanesulfonic acid; water; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; zinc; [2,2]bipyridinyl; N,N-dimethyl-formamide; nickel dibromide; In tetrahydrofuran; methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 39778-63-7
3-(1,1-dimethylethyl)-4-hydroxybenzoic acid methyl ester

: 1285575-37-2
3-t-butyl-4-methoxy-5-methylsulfonylbenzoyl chloride

Guidance literature:: Multi-step reaction with 6 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 0.25 h / 20 °C

2: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C

3: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C

4: 3-chloro-benzenecarboperoxoic acid / chloroform / 3 h / 20 °C

5: lithium hydroxide monohydrate; water / tetrahydrofuran / 5 h / 20 °C

6: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

With N-iodo-succinimide; thionyl chloride; lithium hydroxide monohydrate; trifluorormethanesulfonic acid; water; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; zinc; [2,2]bipyridinyl; N,N-dimethyl-formamide; nickel dibromide; In tetrahydrofuran; methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;