methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

Base Information

Chemical Name:methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate
CAS No.:1285575-30-5
Molecular Formula:C₁₃H₁₈O₃S
Molecular Weight:254.35
Hs Code.:

Synonyms:methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

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Chemical Property of methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

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Technology Process of methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

There total 3 articles about methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 628337-16-6
methyl 3-tert-butyl-4-hydroxy-5-iodobenzoate

: 624-92-0
Dimethyldisulphide

: 1285575-30-5
methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

Guidance literature:: With zinc; [2,2]bipyridinyl; nickel dibromide; In N,N-dimethyl-formamide; at 130 ℃; for 1h;

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1285575-30-5
methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanesulfonic acid / 16 h / 70 °C

1.2: 3 h / 50 °C

2.1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 0.25 h / 20 °C

3.1: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C

With N-iodo-succinimide; methanesulfonic acid; trifluorormethanesulfonic acid; zinc; [2,2]bipyridinyl; nickel dibromide; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 39778-63-7
3-(1,1-dimethylethyl)-4-hydroxybenzoic acid methyl ester

: 1285575-30-5
methyl 3-t-butyl-4-hydroxy-5-methylsulfanylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 0.25 h / 20 °C

2: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; zinc; [2,2]bipyridinyl; nickel dibromide; In methanol; dichloromethane; N,N-dimethyl-formamide;