N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide

Base Information

Chemical Name:N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide
CAS No.:1272718-38-3
Molecular Formula:C₁₆H₁₅F₃INO₂S
Molecular Weight:469.266
Hs Code.:

Synonyms:N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide

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Chemical Property of N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide

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Technology Process of N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide

There total 1 articles about N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 71530-58-0
m-cumenesulfonyl chloride

: 163444-17-5
2-iodo-4-(trifluoromethyl)aniline

: 1272718-38-3
N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide

Guidance literature:: 3-isopropylbenzene-1-sulfonyl chloride; 2-iodo-4-(trifluoromethyl)aniline; With pyridine; at 20 ℃; for 21h;

With water; potassium hydroxide; In 1,4-dioxane; at 20 ℃; for 77h; Reflux;

With hydrogenchloride; In 1,4-dioxane; water; Cooling with ice;

Reference yield:

: 1272718-38-3
N-[2-iodo-4-(trifluoromethyl)-phenyl]-3-(1-methylethyl)benzenesulfonamide

: 1272718-40-7
4-[[1-[[3-(1-methylethyl)phenyl]sulfonyl]-5-(trifluoromethyl)-1H-indol-2-yl]methyl]benzoic acid, methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / Reflux

2.1: trifluoroacetic acid; boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 1 h / 20 °C

2.2: Cooling with ice

With triethylsilane; boron trifluoride diethyl etherate; diethylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In dichloromethane; N,N-dimethyl-formamide; 1.1: Sonogashira Coupling;