5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

Base Information

Chemical Name:5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate
CAS No.:1180003-33-1
Molecular Formula:C₂₀H₂₄BrNO₄S
Molecular Weight:454.385
Hs Code.:

Synonyms:5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

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Chemical Property of 5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

Chemical Property:

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Technology Process of 5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

There total 3 articles about 5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1180003-32-0
N-((S)-1-(4-bromophenyl)-ethyl)-5-hydroxy-3-phenyl-pentanamide

: 124-63-0
methanesulfonyl chloride

: 1180003-33-1
5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;

Reference yield:

: 4160-80-9
3-phenylglutaric acid anhydride

: 1180003-33-1
5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / -78 - 20 °C / Inert atmosphere

2: borane / tetrahydrofuran / 0.5 h / 0 °C

3: triethylamine / dichloromethane / 0 °C

With borane; triethylamine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 27298-97-1
(S)-1-(4-bromophenyl)ethylamine

: 1180003-33-1
5-((S)-1-(4-bromo-phenyl)ethylamino)-5-oxo-3-phenyl-pentyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / -78 - 20 °C / Inert atmosphere

2: borane / tetrahydrofuran / 0.5 h / 0 °C

3: triethylamine / dichloromethane / 0 °C

With borane; triethylamine; In tetrahydrofuran; dichloromethane; toluene;