2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

Base Information

Chemical Name:2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt
CAS No.:952498-24-7
Molecular Formula:C₁₆H₁₃F₃NO₃*K
Molecular Weight:363.378
Hs Code.:

Synonyms:2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

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Chemical Property of 2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

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Technology Process of 2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

There total 6 articles about 2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 927685-43-6
2-hydroxy-5-[2-(4-(trifluoromethylphenyl)ethylamino)]benzoic acid

: 952498-24-7
2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

Guidance literature:: With potassium hydroxide; In ethanol; at 0 - 20 ℃; for 2h; pH=6.8 - 7.0;

Reference yield:

: 130365-87-6
2-[4-(trifluoromethyl)phenyl]ethyl bromide

: 952498-24-7
2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 3 h / 20 °C

2.1: potassium hydroxide / ethanol / 2 h / 0 - 20 °C / pH 6.8 - 7.0

With potassium hydroxide; tetra-(n-butyl)ammonium iodide; triethylamine; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 89-57-6
5-Aminosalicylic Acid

: 952498-24-7
2-hydroxy-5-[2-(4-trifluoromethyl-phenyl)-ethylamino]-benzoic acid potassium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

1.2: 3 h / 20 °C

2.1: potassium hydroxide / ethanol / 0 - 20 °C / pH 6.8 - 7.0

With triethylamine; potassium hydroxide; tetra-(n-butyl)ammonium iodide; In ethanol; N,N-dimethyl-formamide;