3-(4-methoxyphenyl)-2-[4-(methylsulfanyl)phenyl]-2,3-dihydro-4(1H)-quinazolinone

Base Information

Chemical Name:3-(4-methoxyphenyl)-2-[4-(methylsulfanyl)phenyl]-2,3-dihydro-4(1H)-quinazolinone
CAS No.:371118-62-6
Molecular Formula:C₂₂H₂₀N₂O₂S
Molecular Weight:376.479
Hs Code.:
Mol file:371118-62-6.mol

Synonyms:3-(4-methoxyphenyl)-2-(4-(methylthio)phenyl)-1,3-benzdiazinan-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)-2-[4-(methylsulfanyl)phenyl]-2,3-dihydro-4(1H)-quinazolinone

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Technology Process of 3-(4-methoxyphenyl)-2-[4-(methylsulfanyl)phenyl]-2,3-dihydro-4(1H)-quinazolinone

There total 3 articles about 3-(4-methoxyphenyl)-2-[4-(methylsulfanyl)phenyl]-2,3-dihydro-4(1H)-quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 118-48-9
isatoic anhydride

: 22116-70-7
N-(p-Methylmercaptobenzal)-p-anisidin

: 371118-62-6
3-(4-methoxyphenyl)-2-(4-(methylthio)phenyl)-1,3-benzdiazinan-4-one

Guidance literature:: In neat (no solvent); Microwave irradiation;
DOI:10.1016/j.bmc.2012.09.069

Reference yield: 30.0%

: 118-48-9
isatoic anhydride

: 104-94-9
4-methoxy-aniline

: 3446-89-7
4-(Methylthio)benzaldehyde

: 371118-62-6
3-(4-methoxyphenyl)-2-(4-(methylthio)phenyl)-1,3-benzdiazinan-4-one

Guidance literature:: With aluminum potassium sulfate dodecahydrate; In ethanol; for 1h; Reflux;
DOI:10.1002/ardp.201100138

Reference yield:

: 3446-89-7
4-(Methylthio)benzaldehyde

: 371118-62-6
3-(4-methoxyphenyl)-2-(4-(methylthio)phenyl)-1,3-benzdiazinan-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 10 h / 78 °C

2: neat (no solvent) / Microwave irradiation

With acetic acid; In ethanol;
DOI:10.1016/j.bmc.2012.09.069