4-chloro-2-iodophenyl methoxymethyl sulfide

Base Information

Chemical Name:4-chloro-2-iodophenyl methoxymethyl sulfide
CAS No.:1610038-81-7
Molecular Formula:C₈H₈ClIOS
Molecular Weight:314.574
Hs Code.:

Synonyms:4-chloro-2-iodophenyl methoxymethyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-2-iodophenyl methoxymethyl sulfide

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Technology Process of 4-chloro-2-iodophenyl methoxymethyl sulfide

There total 1 articles about 4-chloro-2-iodophenyl methoxymethyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 63069-48-7
p-chloro-o-iodoaniline

: 140-89-6
potassium ethyl xanthogenate

: 1610038-81-7
4-chloro-2-iodophenyl methoxymethyl sulfide

Guidance literature:: p-chloro-o-iodoaniline; With tetrafluoroboric acid; isopentyl nitrite; In ethanol; water; at 0 ℃; for 0.333333h;

potassium ethyl xanthogenate; With isopentyl nitrite; In acetone; at -40 - 0 ℃; for 1.33333h;
DOI:10.1039/c4ob00299g

Reference yield: 83.0%

: 1610038-81-7
4-chloro-2-iodophenyl methoxymethyl sulfide

: 536-74-3
phenylacetylene

: 1610038-73-7
4-chloro-2-(phenylethynyl)phenyl methoxymethyl sulfide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1039/c4ob00299g

Reference yield: 70.0%

: 772-38-3
4-tert-Butylphenylacetylene

: 1610038-81-7
4-chloro-2-iodophenyl methoxymethyl sulfide

: 1610038-74-8
2-[(4-tert-butylphenyl)ethynyl]-4-chlorophenyl methoxymethyl sulfide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1039/c4ob00299g