N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

Base Information

Chemical Name:N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide
CAS No.:1254556-16-5
Molecular Formula:C₁₈H₁₈N₄O₂S₂
Molecular Weight:386.499
Hs Code.:

Synonyms:N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

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Chemical Property of N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

Chemical Property:

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Technology Process of N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

There total 3 articles about N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 58006-91-0
phenyl(phenylaminocarbonyl)carbamate

: 101774-85-0
3-(benzo[d]thiazol-2-ylthio)propan-1-amine

: 1254556-16-5
N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

Guidance literature:: With layered Zn/Cr(III) (3:1 mol ratio)hydroxides attached by hexamethylene-1,6-diisocyanate and citric acid; In dichloromethane; for 1h; Reflux;
DOI:10.1002/bkcs.12152

Reference yield:

: 142-04-1,36663-09-9
aniline hydrochloride

: 1254556-16-5
N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

Guidance literature:: Multi-step reaction with 3 steps

1: water / 25 °C

2: pyridine / dichloromethane / 16 h / 25 °C

3: layered Zn/Cr(III) (3:1 mol ratio)hydroxides attached by hexamethylene-1,6-diisocyanate and citric acid / dichloromethane / 1 h / Reflux

With pyridine; In dichloromethane; water;
DOI:10.1002/bkcs.12152

Reference yield:

: 64-10-8
phenyl carbamate

: 1254556-16-5
N-phenyl-N'-[3-(benzo[b]thiazol-2-ylthio)propyl] imidodicarbonic diamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 16 h / 25 °C

2: layered Zn/Cr(III) (3:1 mol ratio)hydroxides attached by hexamethylene-1,6-diisocyanate and citric acid / dichloromethane / 1 h / Reflux

With pyridine; In dichloromethane;
DOI:10.1002/bkcs.12152