(mesitylene)osmium dichloride

Base Information

Chemical Name:(mesitylene)osmium dichloride
CAS No.:126724-08-1
Molecular Formula:C₉H₁₂*2Cl*Os
Molecular Weight:381.3
Hs Code.:

Synonyms:(mesitylene)osmium dichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (mesitylene)osmium dichloride

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Technology Process of (mesitylene)osmium dichloride

There total 1 articles about (mesitylene)osmium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: osmium(III) chloride trihydrate

: 4074-23-1
1,3,5-trimethylcyclohexane-1,4-diene

: 126724-08-1
(mesitylene)osmium dichloride

Guidance literature:: In ethanol; Ar atmosphere; refluxing (16 h); pptn. on concn. and cooling (0°C, 2 h), removal of mother liquor, washing (ether), drying (vac.); elem. anal.;
DOI:10.1021/om00156a029

Reference yield: 97.0%

: 126724-08-1
(mesitylene)osmium dichloride

: 1197040-29-1,931-54-4
phenyl isocyanate

: 136033-83-5
(mesitylene)(phenylisonitrile)osmium(II) dichloride

Guidance literature:: In dichloromethane; under Ar; a suspn. of ((mes)OsCl2) is treated with the isocyanide; mixt. stirred for 3 h at 40°C; soln. filtered; residue washed (CH2Cl2); filtrate concd.; addn of ether; ppt. filtered, washed (ether/hexane), dried (vac.); elem. anal.;
DOI:10.1021/om00055a053

Reference yield: 94.0%

: 126724-08-1
(mesitylene)osmium dichloride

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 156823-21-1
Os((CH₃)3C₆H₃)((CH₃)2C₆H₃NC)Cl₂

Guidance literature:: In dichloromethane; (Ar); to a suspn. of Os-compd. in CH2Cl2 CNXyl is added, mixt. is stirred for 2.5 h at room temp.; soln. is filtered, residue is washed three times with CH2Cl2, the filtrates are collected and their volumes are reduced, addn. of ether leads to ppt., which is filtered off, washed with ether and dried in vac.; elem. anal.;
DOI:10.1016/0022-328X(94)88074-3