methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

Base Information

Chemical Name:methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate
CAS No.:158302-78-4
Molecular Formula:C₂₇H₃₂O₄
Molecular Weight:420.549
Hs Code.:

Synonyms:methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

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Chemical Property of methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

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Technology Process of methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

There total 6 articles about methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 93940-28-4
3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-2H-anthracen-1-one

: 1571-08-0
methyl 4-formylbenzoate

: 158302-78-4
methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

Guidance literature:: With sodium hydroxide; In methanol; for 24h; Ambient temperature;
DOI:10.1021/jm00016a020

Reference yield:

: 6683-46-1
1,1,4,4-Tetramethyl-1,2,3,4-tetrahydro-naphthalene

: 158302-78-4
methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: AlCl₃ / CH₂Cl₂ / 6 h / Ambient temperature

2: 5 N NaOH / ethanol / 3 h / Ambient temperature

3: NaOH, hydrazine monohydrate, diethylene glycol / 6 h / 140 °C

4: thionyl chloride / benzene / 0.67 h / Heating

5: AlCl₃ / CS₂ / 4 h / Heating

6: 64 percent / NaOH / methanol / 24 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; thionyl chloride; hydrazine hydrate; diethylene glycol; In methanol; carbon disulfide; ethanol; dichloromethane; benzene;
DOI:10.1021/jm00016a020

Reference yield:

: 119028-91-0
4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)butyric acid

: 158302-78-4
methyl 4-<(3,4,5,6,7,8-hexahydro-5,5,8,8-tetramethyl-1(2H)-oxoanthracen-2-yl)hydroxymethyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / benzene / 0.67 h / Heating

2: AlCl₃ / CS₂ / 4 h / Heating

3: 64 percent / NaOH / methanol / 24 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; thionyl chloride; In methanol; carbon disulfide; benzene;
DOI:10.1021/jm00016a020