6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one

Base Information

Chemical Name:6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one
CAS No.:1381869-02-8
Molecular Formula:C₂₀H₂₀Cl₂N₂O₃
Molecular Weight:407.296
Hs Code.:

Synonyms:6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one

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Chemical Property of 6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one

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Technology Process of 6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one

There total 2 articles about 6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1381868-92-3
C₂₃H₂₆Cl₂N₂O₄S₂

: 1381869-02-8
6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one

Guidance literature:: With dilauryl peroxide; dibenzoyl peroxide; In water; ethyl acetate; at 73 - 75 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.04.020

Reference yield:

: 39716-58-0
pent-4-enoyl chloride

: 1381869-02-8
6,8-dichloro-1-methyl-5-(3-oxo-4-phenoxybutyl)-4,5-dihydro-1H-pyrido[4,3-b]azepin-2(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine

2: potassium carbonate / acetone / Sealed vessel

3: dilauryl peroxide / ethyl acetate / Reflux

4: dilauryl peroxide; dibenzoyl peroxide / water; ethyl acetate / 73 - 75 °C / Inert atmosphere

With dilauryl peroxide; potassium carbonate; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In water; ethyl acetate; acetone;
DOI:10.1016/j.tetlet.2012.04.020