C₄₆H₆₄O₁₅Si

Base Information

Chemical Name:C₄₆H₆₄O₁₅Si
CAS No.:256342-15-1
Molecular Formula:C₄₆H₆₄O₁₅Si
Molecular Weight:885.091
Hs Code.:

C<sub>46</sub>H<sub>64</sub>O<sub>15</sub>Si

Synonyms:C₄₆H₆₄O₁₅Si

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Chemical Property of C₄₆H₆₄O₁₅Si

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Technology Process of C₄₆H₆₄O₁₅Si

There total 50 articles about C₄₆H₆₄O₁₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 306726-47-6
C₄₇H₆₂O₁₆Si

: 256342-15-1
C₄₆H₆₄O₁₅Si

Guidance literature:: With methanol; sodium hydroxide; In diethyl ether; at 25 ℃; for 1h;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8

Reference yield:

: 256342-14-0
C₄₆H₆₂O₁₃Si

: C₄₆H₆₄O₁₅Si

: 256342-15-1
C₄₆H₆₄O₁₅Si

Guidance literature:: With Quinuclidine; N-methyl-2-indolinone; water; osmium(VIII) oxide; In acetone; at 25 ℃; for 36h;
DOI:10.1002/(SICI)1521-3773(19991115)38:22<3340::AID-ANIE3340>3.0.CO;2-2

Reference yield:

: 256341-86-3
tert-Butyl-[(3S,4S,5R)-2-fluoro-5-(4-methoxy-benzyloxy)-3-phenylselanyl-tetrahydro-pyran-4-yloxy]-dimethyl-silane

: 256342-15-1
C₄₆H₆₄O₁₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 92 percent / SnCl₂ / diethyl ether / 3 h / 0 - 25 °C

2.1: 98 percent / K₂CO₃; MeOH / diethyl ether / 1 h / 25 °C

3.1: aq. NaIO₄; NaHCO₃ / methanol; CH₂Cl₂ / 2 h / 25 °C

4.1: 430 mg / iPr₂NH; vinyl acetate / toluene / 12 h / 140 °C

5.1: 95 percent / TBAF / tetrahydrofuran / 0.5 h / 0 °C

6.1: 97 percent / Et₃N; DMAP / CH₂Cl₂ / 2 h / 0 - 25 °C

7.1: 95 percent / TBAF; AcOH / tetrahydrofuran / 1 h / 25 °C

8.1: 85 percent / Martin sulfurane; Et₃N / CHCl₃ / 2 h / 50 °C

9.1: 90 percent / K₂CO₃; MeOH / 6 h / 25 °C

10.1: NaH; 18-crown-6 / tetrahydrofuran / 0.25 h / 0 °C

10.2: 80 percent / tetrahydrofuran / 2 h / 0 °C

11.1: NMO; H₂O; OsO₄ / quinuclidine / acetone / 36 h / 25 °C

With methanol; dmap; sodium periodate; osmium(VIII) oxide; vinyl acetate; N-methyl-2-indolinone; Martins sulfurane; 18-crown-6 ether; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; diisopropylamine; tin(ll) chloride; Quinuclidine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; acetone; toluene; 1.1: Glycosidation / 2.1: Deacylation / 3.1: Oxidation / 4.1: Cyclization / 5.1: Silyl ether cleavage / 6.1: Esterification / 7.1: Silyl ether cleavage / 8.1: Dehydration / 9.1: Debenzoylation / 10.1: Metallation / 10.2: Etherification / 11.1: Oxidation;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8