tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane

Base Information

• Chemical Name: tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane
• CAS No.: 173069-15-3
• Molecular Formula: C₂₀H₃₆OSSi
• Molecular Weight: 352.657

Synonyms:tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane

Chemical Property of tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane

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Technology Process of tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane

There total 3 articles about tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

tert-Butyl-dimethyl-[2,3,5,6-tetramethyl-4-(2-methyl-propane-2-sulfinyl)-phenoxy]-silane (173069-08-4) + trifluoroacetic anhydride (407-25-0) → tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane (173069-15-3) + Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester (173069-11-9)

Guidance literature:

In chloroform; at 0 ℃; for 0.5h;

DOI:10.1021/jo970418o

Reference yield:

tert-Butyl-dimethyl-[2,3,5,6-tetramethyl-4-(2-methyl-propane-2-sulfinyl)-phenoxy]-silane (173069-08-4) → tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane (173069-15-3) + Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester (173069-11-9)

Guidance literature:

With trifluoroacetic anhydride; In chloroform-d1; at 0 ℃; for 0.166667h;

DOI:10.1039/c39950002319

Reference yield:

tert-Butyl-dimethyl-(2,3,5,6-tetramethyl-4-thiocyanato-phenoxy)-silane (196944-22-6) → tert-Butyl-(4-tert-butylsulfanyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane (173069-15-3)

Guidance literature:

DOI:10.1021/jo970418o

upstream raw materials:

tert-Butyl-dimethyl-[2,3,5,6-tetramethyl-4-(2-methyl-propane-2-sulfinyl)-phenoxy]-silane

trifluoroacetic anhydride

tert-Butyl-dimethyl-(2,3,5,6-tetramethyl-4-thiocyanato-phenoxy)-silane

Downstream raw materials:

2,3,5,6-Tetramethyl-4-(2-methyl-propane-2-sulfinyl)-phenol

Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester

tert-Butyl-dimethyl-[2,3,5,6-tetramethyl-4-(2-methyl-propane-2-sulfinyl)-phenoxy]-silane

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