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C69H86N2O19

Base Information
  • Chemical Name:C69H86N2O19
  • CAS No.:180154-27-2
  • Molecular Formula:C69H86N2O19
  • Molecular Weight:1247.44
  • Hs Code.:
C<sub>69</sub>H<sub>86</sub>N<sub>2</sub>O<sub>19</sub>

Synonyms:C69H86N2O19

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Chemical Property of C69H86N2O19
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Technology Process of C69H86N2O19

There total 9 articles about C69H86N2O19 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) DMF, -50 deg C, 5 min, 2.) DMF, from 0 deg C to RT, 9 h
2: 96 percent / H2 / 20percent Pd(OH)2/C / ethyl acetate; ethanol / 16 h / 2844.3 Torr
3: CH2Cl2 / 20 h / Ambient temperature
With hydrogen; sodium hydride; palladium dihydroxide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja960274f
Guidance literature:
Multi-step reaction with 4 steps
1: 94 percent / H2 / 10percent Pd/C / methanol / 24 h / 2585.7 Torr
2: 1.) NaH / 1.) DMF, -50 deg C, 5 min, 2.) DMF, from 0 deg C to RT, 9 h
3: 96 percent / H2 / 20percent Pd(OH)2/C / ethyl acetate; ethanol / 16 h / 2844.3 Torr
4: CH2Cl2 / 20 h / Ambient temperature
With hydrogen; sodium hydride; palladium dihydroxide; palladium on activated charcoal; In methanol; ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja960274f
Guidance literature:
Multi-step reaction with 2 steps
1: 96 percent / H2 / 20percent Pd(OH)2/C / ethyl acetate; ethanol / 16 h / 2844.3 Torr
2: CH2Cl2 / 20 h / Ambient temperature
With hydrogen; palladium dihydroxide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja960274f
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