2-(2-chlorophenyl)butanoyl chloride

Base Information

Chemical Name:2-(2-chlorophenyl)butanoyl chloride
CAS No.:1421711-89-8
Molecular Formula:C₁₀H₁₀Cl₂O
Molecular Weight:217.095
Hs Code.:

Synonyms:2-(2-chlorophenyl)butanoyl chloride

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Chemical Property of 2-(2-chlorophenyl)butanoyl chloride

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Technology Process of 2-(2-chlorophenyl)butanoyl chloride

There total 1 articles about 2-(2-chlorophenyl)butanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 188014-56-4
2-chlorophenylbutyric acid

: 1421711-89-8
2-(2-chlorophenyl)butanoyl chloride

Guidance literature:: With thionyl chloride; for 2h; Reflux;
DOI:10.1002/adsc.200800532

Reference yield: 52.0%

: 1421711-89-8
2-(2-chlorophenyl)butanoyl chloride

: 1070793-26-8
2-(2-chlorophenyl)but-1-en-1-one

Guidance literature:: With SEC-BUTYLAMINE; In diethyl ether; at 0 ℃; Inert atmosphere;
DOI:10.1002/chem.201503308

Reference yield:

: 1421711-89-8
2-(2-chlorophenyl)butanoyl chloride

: (R)-2,2-dichlorovinyl 2-chloro-2-(2-chlorophenyl)butanoate

: (S)-2,2-dichlorovinyl 2-chloro-2-(2-chlorophenyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: SEC-BUTYLAMINE / diethyl ether / 0 °C / Inert atmosphere

2: potassium hexamethylsilazane; (S)-5-{[(tert-butyldimethylsilyl)oxy]diphenylmethyl}-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate / toluene / 12 h / 0 °C / Schlenk technique; Inert atmosphere

With SEC-BUTYLAMINE; (S)-5-{[(tert-butyldimethylsilyl)oxy]diphenylmethyl}-2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; potassium hexamethylsilazane; In diethyl ether; toluene;
DOI:10.1002/chem.201503308