N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

Base Information

Chemical Name:N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide
CAS No.:1297587-42-8
Molecular Formula:C₁₉H₂₅N₃O
Molecular Weight:311.427
Hs Code.:

Synonyms:N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

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Chemical Property of N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

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Technology Process of N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

There total 6 articles about N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1207535-65-6
m-[(N-4-dimethylaminobenzyl-N-methyl)aminomethyl]benzylamine

: 109-94-4
formic acid ethyl ester

: 1297587-42-8
N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

Guidance literature:: Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2011.02.026

Reference yield:

: 1207535-64-5
N-[{3-(azidomethyl)phenyl}methyl]-N-(4-dimethylaminobenzyl)methylamine

: 1297587-42-8
N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 6 h / Inert atmosphere; Reflux

2.1: Inert atmosphere; Reflux

With triphenylphosphine; In tetrahydrofuran; 1.1: Staudinger reaction / 1.2: Staudinger reaction;
DOI:10.1016/j.ejmech.2011.02.026

Reference yield:

: 1144106-66-0
1-(azidomethyl)-3-(bromomethyl)benzene

: 1297587-42-8
N-[{3-(N-(4-(dimethylamino)benzyl)-N-methylaminomethyl)phenyl}methyl]formamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 6 h / 0 °C / Reflux

2.1: triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.2: 6 h / Inert atmosphere; Reflux

3.1: Inert atmosphere; Reflux

With potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetonitrile; 2.1: Staudinger reaction / 2.2: Staudinger reaction;
DOI:10.1016/j.ejmech.2011.02.026