(2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

Base Information

Chemical Name:(2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal
CAS No.:238421-68-6
Molecular Formula:C₂₅H₃₄O₄Si
Molecular Weight:426.628
Hs Code.:

Synonyms:(2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

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Chemical Property of (2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

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Technology Process of (2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

There total 3 articles about (2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 238421-67-5
(4R,6S)-4-(tert-butyldiphenylsilyloxymethyl)-5,6-dihydroxy-4,7-dimethyloctanal ethylene acetal

: 238421-68-6
(2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; at 20 ℃; for 6h;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 238421-68-6
(2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

2: 48 percent / NaIO₄ / H₂O; dioxane / 6 h / 20 °C

With dmap; sodium periodate; In 1,4-dioxane; dichloromethane; water; 1: Substitution / 2: Oxidation;

Reference yield:

: (2R,4S)-2-(2-[1,3]Dioxolan-2-yl-ethyl)-2,5-dimethyl-hexane-1,3,4-triol

: 238421-68-6
(2R)-2-(tert-butyldiphenylsilyloxymethyl)-2-methylpentanedial 5-ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

2: 48 percent / NaIO₄ / H₂O; dioxane / 6 h / 20 °C

With dmap; sodium periodate; In 1,4-dioxane; dichloromethane; water; 1: Substitution / 2: Oxidation;