(benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten

Base Information

Chemical Name:(benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten
CAS No.:107557-53-9
Molecular Formula:C₃₁H₂₂O₅S₂SnW
Molecular Weight:841.205
Hs Code.:

Synonyms:(benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten

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Chemical Property of (benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten

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Technology Process of (benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten

There total 2 articles about (benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 14040-11-0
tungsten hexacarbonyl

: 87451-07-8
benzyl triphenylstannanedithiocarboxylate

: 107557-53-9
(benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten

Guidance literature:: With C₄H₈O; In tetrahydrofuran; reaction of the ester with the activated metalcarbonyle in THF under Ar; evapn. of the solvent, chromy. on silicagel (THF/petroleum ether), recrystn. (n-hexane), elem. anal.;

Reference yield: 48.0%

: 36477-75-5
tungsten pentacarbonyl tetrahydrofuran

: 87451-07-8
benzyl triphenylstannanedithiocarboxylate

: 107557-53-9
(benzyl triphenylstannanedithiocarboxylate)pentacarbonyltungsten

Guidance literature:: In tetrahydrofuran; soln. of W complex and Sn compound in THF was stirred under exclusion of light for 2 h;; reduced in vol., recrystd. from n-hexane;;
DOI:10.1016/S0020-1693(00)84371-6